X-ray diffraction equipment

Panoramic view of the X-ray diffractometers of the laboratory

Our laboratory is equipped with several X-ray diffractometers, which cover most of the needs encountered both in routine and in advanced materials science studies. A brief description is given below.

High-resolution XRD

Bruker D8 Discover (2014)

  • Cu Kα1 radiation, Göbel mirror and four-reflection Ge(220) monochromator
  • Six-axis diffractometer (θ, 2θ, χ, φ + double-tilt stage), plus two axes for in-plane diffraction
  • High-temperature heating stage (Anton Paar DHS 1100)
  • One-dimensional LynxEye detector

Total scattering

Customised Siemens P4

  • Refurbished instrument
  • Mo Kα1 radiation with graphite monochromator
  • Capillary sample holder
  • Scintillation counter
  • Custom data acquisition software

Single-crystal diffraction

Nonius Kappa CCD (2001)

  • Mo Kα1 radiation with graphite monochromator
  • Four-circle Eulerian cradle
  • CCD camera

Powder diffraction

Bruker D8 Advance Da Vinci (2015)

  • Cu Kα radiation with Ni filter
  • θ/θ goniometer
  • One-dimensional LynxEye XE-T detector with energy discrimination
  • High-temperature furnace (Anton Paar HTK 1200N)

Powder diffraction

Bruker D8 Advance (2009)

  • Cu Kα1 radiation with focusing Ge monochromator
  • θ/2θ goniometer
  • One-dimensional LynxEye detector

Powder diffraction

Bruker D5000

  • Cu Kα radiation with Ni filter
  • θ/2θ goniometer
  • Point detector with energy discrimination (Sol-X)